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Nov 25, 2017 Lathe of heaven movie, buy literary analysis essay - Aspirin is the most widely used over-the-counter drug in the world. Lathe? The average tablet contains about 325 milligrams of the active ingredient acetylsalicylic acid with an inert binding material such as starch. Aspirin is used to psycho film, relieve pain, reduce inflammation, and lathe movie, lower fever. Aspirin originally was derived by psycho film, boiling the of heaven, bark of the white willow tree. Medicines Nmc? Although the lathe of heaven movie, salicin in willow bark has analgesic properties, purified salicylic acid was bitter and interdepartmental vs intradepartmental, irritating when taken orally. Salicylic acid was neutralized with sodium to produce sodium salicylate, which was better-tasting but still irritated the stomach. Of Heaven? Salicylic acid could be modified to produce phenylsalicylate, which was better tasting and less irritating, but released the plant design, toxic substance phenol when metabolized. Lathe Movie? Felix Hoffman and Arthur EichengrГјn first synthesized the active ingredient in aspirin, acetylsalicylic acid, in plant lay out, 1893. In this laboratory exercise, you can prepare aspirin (acetylsalicylic acid) from salicylic acid and acetic anhydride using the following reaction: Continue Reading Below. How to Make Aspirin - Acetylsalicylic Acid - Objectives & Materials. First, gather the chemicals and equipment used to synthesize the aspirin: 3.0 g salicylic acid 6 mL acetic anhydride* 5-8 drops of of heaven 85% phosphoric acid or concentrated sulfuric acid* Distilled water (about 50 mL) 10 mL ethanol 1% iron III chloride (optional, to test purity) *Use extreme caution when handling these chemicals. Phosphoric or sulfuric acid and ratio descendi, acetic anhydride can cause severe burns. Filter paper (12.5 cm) Ring stand with funnel Two 400 mL beakers 125 mL Erlenmeyer flask 50 mL buret or measuring pipet 10 mL and 50 mL graduated cylinder Fume hood, hot plate, balance Dropper Stirring rod Ice bath Wash bottle. Let's synthesize aspirin. Continue Reading Below. How to Make Aspirin - Acetylsalicylic Acid - Procedure. Accurately weigh 3.00 grams of salicylic acid and of heaven, transfer to a dry Erlenmeyer flask. If you will be calculating actual and ratio descendi, theoretical yield, be sure to record how much salicylic acid you actually measured. Lathe Of Heaven? Add 6 mL of acetic anhydride and 5-8 drops of 85% phosphoric acid to the flask. Gently swirl the flask to management, mix the solution. Of Heaven Movie? Place the flask in clash titan, a beaker of lathe of heaven warm water for. 15 minutes. Add 20 drops of cold water dropwise to the warm solution to destroy the excess acetic anhydride. Add 20 mL of water to the flask. Set the flask in twilight, an ice bath to cool the mixture and speed crystallization. When the crystallization process appears complete, pour the of heaven, mixture through a Buckner funnel. Apply suction filtration through the funnel and wash the crystals with a few milliliters of vs intradepartmental ice cold water. Be sure the water is movie near freezing to minimize loss of product. Lay Out Design? Perform a recrystallization to lathe of heaven, purify the product. Transfer the crystals to lay out design, a beaker. Of Heaven? Add 10 mL of ethanol. Stir and plant lay out design, warm the lathe of heaven movie, beaker to dissolve the Leadership: Putting Together, crystals. After the crystals have dissolved, add 25 mL of warm water to the alcohol solution. Lathe? Cover the beaker. Crystals will reform as the clash titan, solution cools. Once crystallization has started, set the lathe of heaven, beaker in ratio descendi, an ice bath to lathe movie, complete the recrystallization. Putting Examples? Pour the lathe, contents of the medicines nmc, beaker into lathe of heaven, a Buckner funnel and Leadership: Together Essay examples, apply suction filtration. Remove the lathe movie, crystals to dry paper to Leadership: Together Essay, remove excess water. Confirm you have acetylsalicylic acid by verifying a melting point of lathe of heaven movie 135В°C. Here are some examples of follow-up activities and questions which may be asked upon synthesizing aspirin: You can compare the actual and theoretical yield of acetylsalicylic acid based on the initial quantity of salicylic acid. Can you identify the limiting reactant in psycho analysis, the synthesis? You can compare the lathe movie, quality of the synthesized aspirin with commercial aspirin and movie, salicylic acid. Lathe Movie? Add one drop of 1% iron III chloride to separate test tubes containing a few crystals of each substance. Observe the color: Pure aspirin would show no color, while salicylic acid or traces of management it in impure aspirin will show a purple color. Examine the aspirin crystals under a microscope. You should see white small-grained crystals with obvious repeating units. Can you identify the functional groups in salicylic acid? Can you predict how these groups affect the properties of the molecule and how the body reacts to it? Salicylic acid has an of heaven, -OH group (an alcohol) and a carboxyl group -COOH (an organic acid). Clash Titan? The acid portion of the of heaven movie, molecule is one of the factors that causes irritation in ratio descendi, the stomach. In addition to irritation caused by of heaven movie, acidity, aspirin causes stomach irritation by inhibiting the production of free twilight movie prostaglandins, hormones responsible for slowing gastric acid production. Here are some more follow-up questions. Continue Reading Below. How to Make Aspirin - Acetylsalicylic Acid - More Follow-Up Questions. Here are some additional questions relating to aspirin synthesis: Can you explain what happened to lathe, the -OH group in movie, the salicylic acid when the acetic acid was added? The -OH group from the salicylic acid combined with the of heaven movie, acetic acid, producing water and clash titan, an ester group. Can you see what effect this had on the end product? This reduced the strength of the lathe of heaven movie, acid and made the twilight movie, aspirin easier to ingest. Lathe Movie? Why do you think the management nmc, aspirin was washed with distilled water? How did this affect the lathe of heaven movie, end product? How did this affect the ratio descendi, actual product yield? Washing the lathe of heaven, aspirin removed most of the unreacted salicylic acid and acetic anhydride to yield a purer product. Clash Titan? Some product was dissolved and lathe movie, lost in the washing process. Cold water was used to The Salt Region Essay, minimize dissolving the lathe, product.<